Preparation of Al matrix nanocomposites by diluting the composite granules containing nano-SiCp under ultrasonic vibaration
来源期刊：JOURNAL OF MATERIALS SCIENCE TECHNOLOG2018年第9期
论文作者：Shulin Lü Pan Xiao Du Yuan Kun Hu Shusen Wu
文章页码：1609 - 1617
摘 要：In this work, an efficient process by diluting the nano-SiCp/Al composite granules in the molten matrix under ultrasonic vibration（UV） was developed to prepare metal matrix nano-composites（MMNCs）.Millimeter-sized composite granules with high content of SiC particle（8 wt%） were specially fabricated by dry high-energy ball milling（HBM） without process control agent, and then remelted and diluted in molten Al alloy under UV. The MMNCs melt was finally squeeze cast under a squeeze pressure of 200 MPa, Microstructure of the composite granules during dry HBM was investigated, and the effect of UV on microstructure and mechanical properties of the MMNCs was discussed. The results indicate that nano-SiC particles are uniformly distributed in the nano-SiCp/Al composite granules, which are covered by vestures of pure Al. During diluting, nano-SiC particles released from the composite granules are quickly dispersed in the molten matrix by UV within 4 min. Microstructure of MMNCs is significantly refined under UV and squeeze casting, eutectic Si phase modified to fine islands with an average length of 1.4 μm. Tensile strength of the squeeze cast MMNCs with 1 wt% of nano-SiC particles is 269 MPa, which is improved by 25% compared with the A356 alloy matrix.
Shulin Lü，Pan Xiao，Du Yuan，Kun Hu，Shusen Wu
State Key Laboratory of Materials Processing and Die & Mould Technology, Huazhong University of Science and Technology
摘 要：In this work, an efficient process by diluting the nano-SiCp/Al composite granules in the molten matrix under ultrasonic vibration（UV） was developed to prepare metal matrix nano-composites（MMNCs）.Millimeter-sized composite granules with high content of SiC particle（8 wt%） were specially fabricated by dry high-energy ball milling（HBM） without process control agent, and then remelted and diluted in molten Al alloy under UV. The MMNCs melt was finally squeeze cast under a squeeze pressure of 200 MPa, Microstructure of the composite granules during dry HBM was investigated, and the effect of UV on microstructure and mechanical properties of the MMNCs was discussed. The results indicate that nano-SiC particles are uniformly distributed in the nano-SiCp/Al composite granules, which are covered by vestures of pure Al. During diluting, nano-SiC particles released from the composite granules are quickly dispersed in the molten matrix by UV within 4 min. Microstructure of MMNCs is significantly refined under UV and squeeze casting, eutectic Si phase modified to fine islands with an average length of 1.4 μm. Tensile strength of the squeeze cast MMNCs with 1 wt% of nano-SiC particles is 269 MPa, which is improved by 25% compared with the A356 alloy matrix.
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