Synthesis and Characterization of Multi-walled Carbon Nanotube Doped Silica Aerogels
来源期刊：Journal Of Wuhan University Of Technology Materials Science Edition2012年第3期
论文作者：王宝民
文章页码：512 - 515
摘 要：Multi-walled carbon nanotube doped silica aerogels（MWCNT-SAs） were synthesized from a wet gel of well-dispersed MWCNT by one-step solvent exchange/surface modification and ambient pressure drying（APD）. Waterglass was employed as a precursor to prepare wet gel. The content of MWCNT varied from 0 to 15% volume by wet gel. The surface group, thermal stability and microstructure of pure silica aerogel and MWCNT-SAs were investigated by FTIR, DTA, and TEM. Experimental results show that MWCNT-SAs are hydrophobic when the temperature is below 400 ℃, MWCNT-SAs exhibit a mesoporous network structure, and they achieve the largest scale with least shrinkage and lowest density when doped with 5 vol% MWCNT.
王宝民
Institute of Building Materials, School of Civil Engineering, Dalian University of Technology
摘 要：Multi-walled carbon nanotube doped silica aerogels（MWCNT-SAs） were synthesized from a wet gel of well-dispersed MWCNT by one-step solvent exchange/surface modification and ambient pressure drying（APD）. Waterglass was employed as a precursor to prepare wet gel. The content of MWCNT varied from 0 to 15% volume by wet gel. The surface group, thermal stability and microstructure of pure silica aerogel and MWCNT-SAs were investigated by FTIR, DTA, and TEM. Experimental results show that MWCNT-SAs are hydrophobic when the temperature is below 400 ℃, MWCNT-SAs exhibit a mesoporous network structure, and they achieve the largest scale with least shrinkage and lowest density when doped with 5 vol% MWCNT.
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