3－甲氧基－4－哌啶基苯基重氮四氯化锡复盐的合成与表征
来源期刊：中南大学学报(自然科学版)1996年第3期
论文作者：蒋金芝 唐有根 钱东
文章页码：358 - 362
关键词：重氮复盐; 感光试剂; 合成; 表征
Key words：diazonium double salt; photo-sensitire reagent; synthesis; characterization
摘 要：合成了一种新的重氮感光试剂－3－甲氧基－4－哌啶基苯基重氮四氯化锡复盐,讨论了制备过程中的各种影响因素,并得到了最佳合成条件;考察了该化合物的感光性能.通过紫外光谱、红外光谱、核磁共振氢谱和元素分析等手段对合成复盐及2个中间产物进行了结构表征
Abstract: The new diazo photo-sensitive reagent 3-methoxyl-4- piperidinylbenzedi stannic chloride double salt was synthesized.Results were discussed in terms of the effects of the reaction,and the optimum synthetic conditions were obtained.The title compound and two medium products were characterized by means of UV, IR, 1HNMR and elemental analysis etc.
