Effect of scandia on tungsten oxide powder reduction process
来源期刊：Journal of Rare Earths2010年第S1期
论文作者：崔云涛 王金淑 刘伟 王茜
文章页码：202 - 205
摘 要：Scandia doped tungsten powders were prepared by spray drying combined with two-step hydrogen reduction.The particle size of doped tungsten powder,powder morphology and doped tungsten matrix were characterized by scanning electron microscope,X-ray diffrac-tion and laser diffraction particle size analyzer,respectively.The reduction behavior of Sc2O3 doped tungsten oxide and the effect of Sc2O3 on the property of tungsten powder were studied by the temperature programmed reduction.The experimental results showed that the pre-cursor powders prepared by spray drying had spherical shape.The addition of Sc2O3 could decrease the reduction temperature of tungsten oxide.The scandia doped tungsten powder had sub-micrometer size in the range of 0.1 to1 μm and scandium distributed evenly in the powder.By using this kind powder,sub-microstructure cathode matrices with semispherical grains and homogenous distribution of scan-dium were obtained.
崔云涛，王金淑，刘伟，王茜
College of Materials Science and Engineering,Beijing University of Technology
摘 要：Scandia doped tungsten powders were prepared by spray drying combined with two-step hydrogen reduction.The particle size of doped tungsten powder,powder morphology and doped tungsten matrix were characterized by scanning electron microscope,X-ray diffrac-tion and laser diffraction particle size analyzer,respectively.The reduction behavior of Sc2O3 doped tungsten oxide and the effect of Sc2O3 on the property of tungsten powder were studied by the temperature programmed reduction.The experimental results showed that the pre-cursor powders prepared by spray drying had spherical shape.The addition of Sc2O3 could decrease the reduction temperature of tungsten oxide.The scandia doped tungsten powder had sub-micrometer size in the range of 0.1 to1 μm and scandium distributed evenly in the powder.By using this kind powder,sub-microstructure cathode matrices with semispherical grains and homogenous distribution of scan-dium were obtained.
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