Characterization of Fe₃Si-based coatings on low silicon steel by pulsed Nd:YAG laser cladding

Dan-yang Dong1,2),Chang-sheng Liu1),Sui-yuan Chen1),Bin Zhang1) 1) Key Laboratory for Anisotropy and Texture of Materials of the Ministry of Education of China,Northeastern University,Shenyang 110004,China 2) School of Science College,Northeastern University,Shenyang 110004,China

Õª Òª£ºThe Fe3Si based coating was produced on the Fe-1Si steel surface by a pulsed Nd:YAG £¨yttrium aluminum garnet£© laser. Its phase constitution and microstructure were characterized by using X-ray diffraction £¨XRD£©,optical microscope £¨OM£©,and field emission scanning electron microscope £¨FESEM£© with associated energy dispersive spectroscopy £¨EDS£© and transmission electron microscopy £¨TEM£©. The hyperfine structure of the coating was studied by MûÖssbauer spectra £¨MS£© and the magnetic property was also measured at room temperature by a vibrating sample magnetometer £¨VSM£©. The obtained coating is pore and crack-free with dense microstructure and high Si content. The metallurgical bonding between the coating and the substrate was realized. The micro-structure of the coating is typical fine dendrites. The major phase was confirmed by XRD and TEM to be the ordering D03 structured Fe3Si phase. In addition,there were smaller amounts of the Fe5Si3 phase and the ¦Ã-Fe phase in the coating. Compared with the substrate,the laser cladding coating has a lower saturation magnetization and a higher coercive force. The poor magnetic property might be because of rapid solidification microstructure and phase constitution in the coating.

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