Healing Process of Casting Pores in a Ni-based Superalloy by Hot Isostatic Pressing
来源期刊：JOURNAL OF MATERIALS SCIENCE TECHNOLOG2015年第11期
论文作者：X.G.Zheng Y.-N.Shi L.H.Lou
文章页码：1151 - 1157
摘 要：Hot isostatic pressing（HIP） with a pressure of 180 MPa at a temperature of 1170 °C was introduced to an investment cast Ni-based superalloy（M91） turbocharger blade to explore the healing process of casting pores generated during investment casting. Optical micrograph and scanning electron microscopy（SEM）observations indicate that eutectic pores are the main cast defects in the as-cast blade before HIP. These pores normally locate at the solidification front of γ/γ′ eutectic with a size of a few micrometers to a few tens of micrometers. After HIP for 4 h, most of the pores were closed. Based on phase characteristics,these pores were healed by the formation of γ matrix with finer and irregular-shaped γ′ precipitates. Healing interface can be easily distinguished by SEM. Line scan by using energy dispersive X-ray spectroscopy（EDS） reveals a much higher Ti and Al concentration in the healing interface. It is proposed that solute diffusion toward the casting pores during HIP results in the formation of γ, and the much higher concentration of γ′-forming elements Al and Ti near the healing interface contributes to the precipitation of γ′ in the healed region in the succeeding cooling process after HIP.
X.G.Zheng1，Y.-N.Shi1，L.H.Lou2
1. Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences2. Superalloy Division, Institute of Metal Research, Chinese Academy of Sciences
摘 要：Hot isostatic pressing（HIP） with a pressure of 180 MPa at a temperature of 1170 °C was introduced to an investment cast Ni-based superalloy（M91） turbocharger blade to explore the healing process of casting pores generated during investment casting. Optical micrograph and scanning electron microscopy（SEM）observations indicate that eutectic pores are the main cast defects in the as-cast blade before HIP. These pores normally locate at the solidification front of γ/γ′ eutectic with a size of a few micrometers to a few tens of micrometers. After HIP for 4 h, most of the pores were closed. Based on phase characteristics,these pores were healed by the formation of γ matrix with finer and irregular-shaped γ′ precipitates. Healing interface can be easily distinguished by SEM. Line scan by using energy dispersive X-ray spectroscopy（EDS） reveals a much higher Ti and Al concentration in the healing interface. It is proposed that solute diffusion toward the casting pores during HIP results in the formation of γ, and the much higher concentration of γ′-forming elements Al and Ti near the healing interface contributes to the precipitation of γ′ in the healed region in the succeeding cooling process after HIP.
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