简介概要

Particular properties of Ti2O and TiNx nanoparticles prepared by thermal decomposition

来源期刊:Rare Metals2008年第6期

论文作者:LI Xiongping, WU Jieda, WEN Ming, TANG Xiao, and LIU Yongqiang Department of Chemistry, Tongji University, Shanghai , China

文章页码:598 - 602

摘    要:Particular properties of Ti2O and TiNx prepared by thermal decomposition were introduced. A precursor prepared by titanium powder react- ing with oxalate acid was thermally decomposed in nitrogen atmosphere at 840°C for 15 min, and relatively pure Ti2O was then obtained. Conductive TiNx was also prepared after altering reaction conditions. Samples were characterized by resistivity, X-ray powder diffraction, transmission electron microscope, Ultraviolet-Visible diffuse reflection, and electromagnetic shielding efficiency. The results indicate that both Ti2O and TiNx have good conductivity. Moreover, Ti2O shows a better solar photocatalytic activity and TiNx does well in the electro- magnetic shield.

详情信息展示

Particular properties of Ti2O and TiNx nanoparticles prepared by thermal decomposition

LI Xiongping, WU Jieda, WEN Ming, TANG Xiao, and LIU Yongqiang Department of Chemistry, Tongji University, Shanghai 200092, China

摘 要:Particular properties of Ti2O and TiNx prepared by thermal decomposition were introduced. A precursor prepared by titanium powder react- ing with oxalate acid was thermally decomposed in nitrogen atmosphere at 840°C for 15 min, and relatively pure Ti2O was then obtained. Conductive TiNx was also prepared after altering reaction conditions. Samples were characterized by resistivity, X-ray powder diffraction, transmission electron microscope, Ultraviolet-Visible diffuse reflection, and electromagnetic shielding efficiency. The results indicate that both Ti2O and TiNx have good conductivity. Moreover, Ti2O shows a better solar photocatalytic activity and TiNx does well in the electro- magnetic shield.

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