Effect of Sintering Time on Structure and Properties in CuO-doping KNN-LS-BF Piezoelectric Ceramics
来源期刊：Journal Of Wuhan University Of Technology Materials Science Edition2019年第2期
论文作者：王华 ZHAI Xia XU Jiwen YANG Ling
文章页码：308 - 311
摘 要：The 0.6 mol% CuO-doping 0.996(0.95 Na0.5K0.5NbO3-0.05 LiSbO3)-0.004 FeBiO3（KNN-LSBF-CuO） piezoelectric ceramics were synthesized by a solid-state reaction technique, and the structure and piezoelectric properties dependence of sintering time in KNN-LS-BF-CuO ceramics were studied. It is found that all the samples sintered for various time are perovskite structure mixed with orthorhombic symmetry phase and tetragonal phase, but the sintering time has significant influences on the crystalline and properties. When the sintering time increases from 2 hours to 6 hours, the grain of KNN-LS-BF-CuO ceramics becomes more homogeneous and more tight-arrangement. The experimental results reveal that the longer sintering time than 4 hours is beneficial for improving partial properties, such as d33, tgδ, and Qm, but is adverse to εr and kp, the KNNLS-BF-CuO ceramics with optimum properties can be synthesized for 6 hours at 1 060 ℃.
王华，ZHAI Xia，XU Jiwen，YANG Ling
School of Materials Science and Engineering, Guilin University of Electronic Technology
摘 要：The 0.6 mol% CuO-doping 0.996(0.95 Na0.5K0.5NbO3-0.05 LiSbO3)-0.004 FeBiO3（KNN-LSBF-CuO） piezoelectric ceramics were synthesized by a solid-state reaction technique, and the structure and piezoelectric properties dependence of sintering time in KNN-LS-BF-CuO ceramics were studied. It is found that all the samples sintered for various time are perovskite structure mixed with orthorhombic symmetry phase and tetragonal phase, but the sintering time has significant influences on the crystalline and properties. When the sintering time increases from 2 hours to 6 hours, the grain of KNN-LS-BF-CuO ceramics becomes more homogeneous and more tight-arrangement. The experimental results reveal that the longer sintering time than 4 hours is beneficial for improving partial properties, such as d33, tgδ, and Qm, but is adverse to εr and kp, the KNNLS-BF-CuO ceramics with optimum properties can be synthesized for 6 hours at 1 060 ℃.
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