New Steel Making Process through Reduction and Sintering of Cementite Powder
来源期刊：材料热处理学报2004年第5期
论文作者：N.OUCHIDA T.TSUCHIYAMA K.NAKASHIMA S.TAKAKI M.EGASHIRA
关键词：cementite; powder metallurgy; reduction; sintering; hydrogen;
摘 要：A new steel making process through reduction and sintering treatment of cementite powder was proposed, and microstructure of the material obtained by this process was examined by scanning electron microscopy and EBSP analysis.The cementite powder obtained by mechanical alloying was compacted under high pressure up to 1000MPa, and then reduced during sintering in a hydrogen (H2) gas atmosphere at elevated temperatures. The cementite compacts were completely reduced by the sintering at 1073K to 1273K for 18ks. The relative density of sintered material became 95% or more when the temperature was elevated above 1173K. The SEM observation and EBSP analysis indicated that the obtained steel has equiaxed ferrite-pearlite structure with grain size of around 5μm and the crystallographic orientations of ferrite grains are randomly distributed.
N.OUCHIDA1，T.TSUCHIYAMA1，K.NAKASHIMA1，S.TAKAKI1，M.EGASHIRA2
(1.Department of Materials Science and Engineering, Kyushu University;
2.Sumitomo Metal Industries, Ltd)
摘要:A new steel making process through reduction and sintering treatment of cementite powder was proposed, and microstructure of the material obtained by this process was examined by scanning electron microscopy and EBSP analysis.The cementite powder obtained by mechanical alloying was compacted under high pressure up to 1000MPa, and then reduced during sintering in a hydrogen (H2) gas atmosphere at elevated temperatures. The cementite compacts were completely reduced by the sintering at 1073K to 1273K for 18ks. The relative density of sintered material became 95% or more when the temperature was elevated above 1173K. The SEM observation and EBSP analysis indicated that the obtained steel has equiaxed ferrite-pearlite structure with grain size of around 5μm and the crystallographic orientations of ferrite grains are randomly distributed.
关键词:cementite; powder metallurgy; reduction; sintering; hydrogen;
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