Synthesis and Characterization of NiFe2O4 Magnetic Nanoparticles by Combustion Method
来源期刊：JOURNAL OF MATERIALS SCIENCE TECHNOLOG2013年第1期
论文作者：M.Kooti A.Naghdi Sedeh
文章页码：34 - 38
摘 要：Magnetic nanoparticles of nickel ferrite （NiFe2O4 ） have been successfully synthesized by microwave-assisted combustion method using stable ferric and nickel salts as precursors and glycine as fuel. The as-synthesized samples were characterized by Fourier transform infrared spectroscopy （FT-IR）, X-ray diffraction （XRD）, transmission electron microscopy （TEM）, vibrating sample magnetometer （VSM） and field emission scanning electron microscopy （FESEM）. The effect of different dose of glycine on the structural parameters and magnetic properties of the prepared NiFe2O4 nanoparticles was also investigated. This study revealed that it was possible to produce larger size of nanoparticles with lower saturation magnetization by using higher dose of fuel.
M.Kooti，A.Naghdi Sedeh
Chemistry Department, College of Science, Shahid Chamran University
摘 要：Magnetic nanoparticles of nickel ferrite （NiFe2O4 ） have been successfully synthesized by microwave-assisted combustion method using stable ferric and nickel salts as precursors and glycine as fuel. The as-synthesized samples were characterized by Fourier transform infrared spectroscopy （FT-IR）, X-ray diffraction （XRD）, transmission electron microscopy （TEM）, vibrating sample magnetometer （VSM） and field emission scanning electron microscopy （FESEM）. The effect of different dose of glycine on the structural parameters and magnetic properties of the prepared NiFe2O4 nanoparticles was also investigated. This study revealed that it was possible to produce larger size of nanoparticles with lower saturation magnetization by using higher dose of fuel.
关键词：
