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Trans. Nonferrous Met. Soc. China 25(2015) 2095-2102 Electrosynthesis of Al/Pb/α-PbO2 composite inert anode materials Gang HU1,2, Rui-dong XU1,2, Shi-wei HE2, Bu-ming CHEN2, Hai-tao YANG3, Bo-hao YU2... of Sciences, Beijing 100190, China Received 16 August 2014; accepted 10 January 2015 Abstract: The α-PbO2 deposition layers were prepared on the surface of Al/Pb substrates by constant current electrosynthesis......
shortened the incubation time for passivity breakdown and accelerated the pit nucleation and growth. The experimental results were helpful to obtain the optimum conditions for electrosynthesis... distillation. In Russia, the electrosynthesis technique has been successfully employed for the commercial production of alkoxides of Y, Ti, Zr, Nb, Ta, Mo, W, Cu, Ge and Sn [8]. To synthesize zirconium......
the solvothermal method. The cyclic voltammetry reveals that the electrosynthesis reaction is irreversible and controlled by the diffusion. The experiments on methylorange degradation show that the unique... and desorption isotherms of MOF-5 and MOF-5(IL) 3.6 Process of electrosynthesis reaction To study the electrochemical synthesis of MOF-5(IL), cyclic voltammetry is performed using standard......
of The Electrochemical Society, 1996, 143(11): 3616-3629. [15] MUNICHANDRAIA N, SATHYANARAYANA S. Insoluble anode of α-lead dioxide coated on titanium for electrosynthesis of sodium perchlorate [J]. Journal..., 2003, 87(4): 599-605. [17] ABACI S, TAMER U, PEKMEZ K, YILDIZ A. Electrosynthesis of 4,4′-dinitroazobenzene on PbO2 electrodes [J]. Journal of Applied Electrochemistry, 2002, 32(2): 193-196. [18] ABACI S......
for the electrosynthesis of Ti-Ge intermetallics from oxides precursors is illustrated in Fig. 2. The experiments were performed under an atmosphere of highly purified argon gas. Pre-electrolysis process was carried out... °C. Fig. 2 Schematic illustration of electrodeoxidation process for electrosynthesis of Ti-Ge intermetallics from oxides (TiO2/GeO2) precursors The phase composition of the starting materials......
Sources, 2007, 168(1): 105?109. [2] ABACI S, TAMER U, PEKMEZ K, YILDIZ A. Electrosynthesis of benzoquinone from phenol on α and β surfaces of PbO2[J]. Electrochimica Acta, 2005, 50(18): 3655?3659. [3] COUPER A M, PLETCHER D, WALSH F C. Electrode materials for electrosynthesis[J]. Chemical Reviews, 1990, 90(5): 837?865. [4] AMADELLI R, De BATTISTI A, GIRENKO D V, KOVALYOV S V, VELICHENKO A B......
T V, DANILOV F I. Composite PbO2-TiO2 materials deposited from colloidal electrolyte: Electrosynthesis, and physicochemical properties [J]. Electrochim Acta, 2009, 54(22): 5239-5245. [6] DAN Yuan... on electrodepositing alpha-lead dioxide coating on aluminum substrate [J]. Acta Chimica Sinica, 2009, 22(5): 373-382. [20] CHEN Bu-ming, GUO Zhong-cheng, XU Rui-dong. Electrosynthesis and physicochemical......
electrode. The electrosynthesis and electrodeposition processes were carried out by the pulse galvanostatic system (Handan Instrument Factory, China) using a two-electrode cell. The cyclic voltammetry(CV...-fei. The electrosynthesis of PANI by pulse galvanostatic method [J]. Chemical Journal of Chinese Universities, 2003, 24(6): 1118-1121. (in Chinese) [14] HUANG B X, TORNATORE P, LI Y S. IR and Raman......
-stable ionic liquids: new and efficient media for electrosynthesis of functional siloxanes[J]. Chem Commun, 2004(6): 674-675. [15] LI Mei-chao, MA Chun-an, LIU Bao-you, et al. A novel electrolyte......
: 589-599. [9] INDIRA L, DIXIT M, KAMATH P V. Electrosynthesis of layered double hydroxides of nickel with trivalent cations [J]. Journal of Power Sources, 1994, 52(1): 93-97. [10] WANG C Y, ZHONG S......