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to the reaction between Ti and O in air, which ultimately leads to the developing of TiO phase. The mass fraction of TiN phase in the coating can be measured by using MDI Jade software and theoretical......
.采用恒电流间隙滴定技术(GITT)研究了Li+动力学扩散情况,在恒电流密度0.1C下对电池充电0.5 h,然后弛豫静置3 h达到近平衡状态,并一直重复该步骤直到上限电压4.3 V. 2 结果与讨论 图1所示为制得材料的XRD谱.用Jade 6.0软件对样品进行物相分析,可发现复合材料中的主要衍射峰都可以很好地与空间群为Rm的层状相LiMO2 (M=Ni, Co, Mn)材料[18]和空......
a D2500 diffractometer with Cu Kα radiation at a scanning step of 0.01°. The parameters of XRD patterns for the tungsten samples were calculated by the software of Jade 6. Dislocation density......
phases are summarized in Tables 1 and 2, which are calculated based on the XRD analysis using Jade 6.0 software and the error of calculation is <0.2%. Obviously, they reduce with increasing Y content......
, Rigaku-TTRIII, Cu Kα) with a scan step of 10 (°)/min, in the 2θ range from 5° to 70°. The XRD pattern was analyzed with MDI JADE software. The concentration of gallium in the leachate was analyzed......
速率为6 (°)/min,扫描范围2θ为10°~90°,分析软件为Jade 8.0.使用瑞士梅特勒公司ASAP2020型物理吸附仪对GAAR和高温颗粒比表面积和介孔孔径进行分析,采用BET法计算比表面积,采用BJH法计算孔径.分析前将2种颗粒吸附剂置于200 ℃下脱气2 h(以上检测项目均由北京中科百测技术服务有限公司提供技术支持),数据拟合和分析均使用Origin 9.1. 1.4  ......
tube using a Sol-X detector. The X-ray diffraction patterns were performed from 10° to 80° at a step size of 0.04° of 2θ and a scan rate of 1°/min. XRD data analysis used the Materials Data Jade 6.0......
极,电流控制在0.1 A/cm2附近. X射线峰形分析在Rigaku D/max 2500PC型衍射仪上执行,工作电压和电流分别为40 kV和150 mA.检测面为轧面(ND面)并靠近样品1/4厚度区域.采用步进扫描记录(200)和(222)晶面衍射峰,步长为0.01°,每步停留1 s,通过JADE 7.0将所得衍射峰进行背底和仪器校正,获得衍射峰宽化数据,在此基础上对不同取向晶粒的储存能进行了分......
Empyrean) using Jade 5.0 of Material Data, Inc. (MDI). The surface structure was analyzed by X-ray photoelectron spectra (XPS, PHI-5702, Al Kα X-ray radiation). A Pyris Diamond thermogravimetric......
Jade分别对两种结构试样的上下层的XRD谱进行分析,发现A型结构的下致密层相较于上致密层向高角度偏移,说明过快的冷却速度使更多的Al,V原子以固溶体的形式存在,而C型结构的上下致密层无明显差异;通过对XRD衍射峰半高宽的统计发现,A型结构下致密层衍射峰的半高宽大于上致密层,说明下致密层具有较细的晶粒,C型结构也有类似的现象,但没有A型结构明显. 上下致密层的维氏硬度测试结果如图10所示,可以看出A,B......