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the width of the prominent peak (311) and the lattice parameter a was refined using Jade 5 software program. As depicted in Table 1, the average crystallite size and the lattice parameter increase......
定.X射线衍射(XRD)测试时使用Cu靶Kα射线,电压40 kV,电流200 mA,扫描角度为10°~90°,扫描速度为4 (°)/min.最后利用Jade 6.0软件进行物相定性和定量分析,定量分析使用Jade 6.0软件中WPF refinement进行全谱拟合精修. 1.4 耐蚀性检测 1.4.1 中性盐雾试验 依照国标GB/T 10125-2012对中性盐雾试验......
为1?4.电沉积过程中使用氨基磺酸溶液和碱式碳酸镍溶液稳定镀液的pH值.沉积3 h后,制备的镍钴合金镀层厚度为180~200 μm,采用机械法剥离镀层. 采用荷兰Philips-FEI公司生产的XL30ESEM? TMP型环境扫描电镜自带的能谱仪测量镍钴合金的成分.采用日本岛津的XD?SA型X射线衍射仪分析镍钴合金镀层的微观结构,衍射条件为铜靶,运用Jade 5.0软件根据XRD谱计算晶粒尺寸......
片,参比电极为饱和甘汞电极(SCE),扫描速度为2 mV/s. 腐蚀产物(漂浮物与沉淀)过滤,烘干后,研磨成粉末,然后采用DMAX?2000的X射线仪对其进行物相检测.测量条件为:Cu靶,石墨单色器滤波,管电压35 kV,管电流50 mA,扫描范围为20?~80?.测量中采用连续扫描,扫描速度为8(?)/min.采用X射线分析软件MID Jade 5.0对实验所得的X射线谱进行分析. 利用......
从镀层上切割拉伸试样.试样总长40 mm,标距区长10 mm,宽6 mm.在微机控制的电子万能试验机(CMT-6104)上进行室温下的单向拉伸试验,应变速率为10-4 s-1.采用日本岛津的XD-SA型X射线衍射仪对镀层结构进行分析,衍射条件为铜靶,电子加速电压为35 kV,电流为20 mA.运用Jade 5.0软件计算微纳米镍的晶粒尺寸与晶格应变,计算前采用经退火处理的标准粗晶硅样品的谱图扣除衍......
by software of Jade 6.0. It can be derived from Table 1 that melt spinning produces broader diffuse peaks, indicating the refinement of the average grain size and stored stress in the grains. The lattice......
相组成.在XRD谱上对金红石相标定时发现,钛阳极1的特征衍射峰形略显不规则,经低速扫描发现其(101)Rutile衍射峰为不对称的峰形(图1(b)),通过Jade软件可以定出一个相为IrO2金红石相,它对应的是处于内层的Ir-Ta二元氧化物涂层(表2).由于该(101)Rutile衍射峰的不对称性,我们认为,在钛阳极涂层中还存在一个以TiO2为基的金红石相固溶体,它的峰位应该在图中虚线所指的位置附......
sample (from JADE card). When orientation factor f equals 1, the degree of orientation for (hkl) is complete; on the other end, complete random state is shown by f = 0 [20]. The value of f for (211......
, which were calculated from the XRD data by the software of Jade 5, are listed in Table 1. The results in Table 1 indicates that the substitution of Cu for Ni obviously enlarges the lattice parameters......
monochromator operated at 40 kV and 200 mA. 2θ was between 20?and 60? with data collection step of 0.02?. The materials data Inc. software JADE 5.0 and the powder diffraction file were used for the phase......