Synthesis of rod-like ultrafine K4Ce2Nb10O30 via a salt-assistant stearic acid method
来源期刊：JOURNAL OF RARE EARTHS2011年第7期
论文作者：朱俊武 马俊兴 吴继科 杨绪杰 陆路德 汪信
文章页码：664 - 667
摘 要：A salt-assistant stearic acid method （SAM） capable of forming ultrafine K4Ce2Nb10O30 products was described. XRD pattern re-vealed that tetragonal K4Ce2Nb10O30 products could be obtained by heat treatment at 900 ℃ for 2 h. Transmission electron microscopy （TEM） observations indicated the introduction of KCl could lead to the formation of rod-like K4Ce2Nb10O30 products. The species of salts played a crucial role in fine tuning the shapes and sizes of K4Ce2Nb10O30 products. Furthermore, the K4Ce2Nb10O30 prepared by salt-assistant SAM had considerable activity under visible light irradiation.
朱俊武，马俊兴，吴继科，杨绪杰，陆路德，汪信
Key Laboratory of Soft Chemistry and Functional Materials, Ministry of Education, Nanjing University of Science and Technology
摘 要：A salt-assistant stearic acid method （SAM） capable of forming ultrafine K4Ce2Nb10O30 products was described. XRD pattern re-vealed that tetragonal K4Ce2Nb10O30 products could be obtained by heat treatment at 900 ℃ for 2 h. Transmission electron microscopy （TEM） observations indicated the introduction of KCl could lead to the formation of rod-like K4Ce2Nb10O30 products. The species of salts played a crucial role in fine tuning the shapes and sizes of K4Ce2Nb10O30 products. Furthermore, the K4Ce2Nb10O30 prepared by salt-assistant SAM had considerable activity under visible light irradiation.
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