超细CaZrO3粉体的湿法制备
来源期刊:中南大学学报(自然科学版)1997年第1期
论文作者:王开毅 陈良 赖德勇 张昭 段桂华 陈小毅
文章页码:94 - 97
关键词:锆酸钙;粉体;超细;湿化学
Key words:calcium zirconate;powder;superfine;wet-chemical
摘 要:CaZrO3粉体是电子陶瓷工业生产和科研中的重要原料之一.作者针对干法合成CaZrO3困难这一实际问题,采用先共沉淀后煅烧的湿法制备技术,并利用化学分析、离心沉降法和透视电镜照相(TEM)等检测手段探讨了工艺条件.实验结果表明,采用湿法可制备颗粒均匀、粒径小于0.5μm、纯度在99.0%以上的CaZrO3粉体.
Abstract: CaZrO3 powder is a kind of important raw materials in the electronic ceramic industry. This paper mainly talks about synthesis of superfine CaZrO3 ceramic powder by means of wet-chemical method. We used such analytic methods as chemical analysis, acentric deposition analysis and transmission electron microscope analysis to make clear the best conditions of synthesis. All the results told us that using this method we could acquire CaZrO3 powder whose average article size is below 0.5 μm with a good dispersion state.