Sol-gel synthesis and photoluminescence characterization of La2Ti2O7:Eu3+ nanocrystals
来源期刊:Rare Metals2011年第6期
论文作者:CHENG Hua,LU Zhouguang,LIU Ying,YANG Haihua,GU Yingying,LI Wei,and TANG Yougen College of Chemistry & Chemical Engineering,Central South University,Changsha ,China
文章页码:602 - 606
摘 要:Eu3+ doped La2Ti2O7 nanocrystals with pure monoclinic phase and size of about 100 nm were prepared by a citric acid(CA) assisted sol-gel method.Techniques of thermo-gravimetric(TG) and differential scanning calorimetry(DSC) ,X-ray diffraction(XRD) ,as well as transmis-sion electron microscopy(TEM) were employed to characterize the as-synthesized nanoparticles.Furthermore,photoluminescence(PL) performances of the Eu3+ doped La2Ti2O7 nanocrystals were evaluated with focus on the effects of calcination temperature and Eu3+ doping concentration on the photoluminescence properties.
CHENG Hua,LU Zhouguang,LIU Ying,YANG Haihua,GU Yingying,LI Wei,and TANG Yougen College of Chemistry & Chemical Engineering,Central South University,Changsha 410083,China
摘 要:Eu3+ doped La2Ti2O7 nanocrystals with pure monoclinic phase and size of about 100 nm were prepared by a citric acid(CA) assisted sol-gel method.Techniques of thermo-gravimetric(TG) and differential scanning calorimetry(DSC) ,X-ray diffraction(XRD) ,as well as transmis-sion electron microscopy(TEM) were employed to characterize the as-synthesized nanoparticles.Furthermore,photoluminescence(PL) performances of the Eu3+ doped La2Ti2O7 nanocrystals were evaluated with focus on the effects of calcination temperature and Eu3+ doping concentration on the photoluminescence properties.
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