Preparation of Nano-SiO2/Amino-modified Polysiloxane Hybrid Superhydrophobic Coating and Thermal-stability Characterization
来源期刊:Journal Of Wuhan University Of Technology Materials Science Edition2014年第1期
论文作者:李金桦 翁睿
文章页码:35 - 39
摘 要:We put forward a large-area and cost-effective method to fabricate superhydrophobic coating by introducing in-situ functionalized nano-SiO2 into side-amino modified hydroxy-terminated polydimethylsiloxane(SA-HTPDMS) curing system. With the characterization using water contact angle(WCA) tester, Fourier transform infrared spectroscopy(FTIR), scanning electron microscope(SEM), atomic force microscopy(AFM) and simultaneous thermal analysis, the as-prepared coating displayed a tremendous WCA of 154.8±1°, sliding angle(SA) about 3.5° and stable self-cleaning property range from-10 to 80 ℃. It was also found that the synergistic effect of surface micro-nano hierarchical structure and chemical hydrophobicity, stability from matrix had made contributions to the superhydrophobicity and excellent heat resistance up to 300 ℃.
李金桦,翁睿
School of Materials Science and Engineering, Wuhan University of Technology
摘 要:We put forward a large-area and cost-effective method to fabricate superhydrophobic coating by introducing in-situ functionalized nano-SiO2 into side-amino modified hydroxy-terminated polydimethylsiloxane(SA-HTPDMS) curing system. With the characterization using water contact angle(WCA) tester, Fourier transform infrared spectroscopy(FTIR), scanning electron microscope(SEM), atomic force microscopy(AFM) and simultaneous thermal analysis, the as-prepared coating displayed a tremendous WCA of 154.8±1°, sliding angle(SA) about 3.5° and stable self-cleaning property range from-10 to 80 ℃. It was also found that the synergistic effect of surface micro-nano hierarchical structure and chemical hydrophobicity, stability from matrix had made contributions to the superhydrophobicity and excellent heat resistance up to 300 ℃.
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